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Publications:

Block II Chemical Biological Mass Spectrometer (CBMS) Program


Complex Aerosol Characterization

Amy B. Dindal, Michelle V. Buchanan, Roger A. Jenkins, and Charles K. Bayne, "Determination of Cocaine and Heroin Vapor Pressures using Commercial and Illicit Samples" The Analyst, 125, 1393-96, 2000

B.Y.H. Liu, F. J. Romay, V. A. Marple, B. A. Olson, D. Roberts, and R. A. Jenkins "Development of an Aerosol Concentrator for Bio-Detection" Presented at the 1999 Scientific Conference on Obscuration and Aerosol Research, Aberdeen Proving Ground, Maryland June 15 - 17, 1999

Amy B. Dindal, Cheng Yu Ma, J. Todd Skeen, and Roger A. Jenkins, "Novel Calibration Technique for Headspace Analysis of Semi-volatile Compounds," Journal of Chromatography A, 793 397 - 402, 1998

Ralph H. Ilgner, Andi Palausky, Roger A. Jenkins, Ann M. Ball, and William E. Lucke, "Distribution of Fatty Acids and Triethanolamine in Synthetic Metalworking Fluid Aerosols Generated in the Laboratory and Field," Presented at the AAMA Metalworking Fluids Symposium, Dearborn, MI, September 15 - 17, 1997

Roger A. Jenkins, "Personal Exposure Monitoring of Complex Atmospheres: Observations and Experiences." Presented at: Ambient Air Quality: Problems and Solutions" Caracas, Venezuela May 6, 1997, (Invited)

Cheng-Yu Ma, J. Todd Skeen, Amy B. Dindal, Charles K. Bayne, and Roger A. Jenkins; "Performance Evaluation of a Thermal Desorption /Gas Chromatography/Mass Spectrometric Method for the Characterization of Waste Tank Headspace Samples," Environmental Science and Technology, 31, 853 859 (1997).

Ralph H. Ilgner, Roger A. Jenkins, C.H. Ho, Ann M. Ball, and William E. Lucke, "Characterization of Coolant Fluid Mists from a Weld Quenching Operation," Proceedings of The Industrial Metal Working Environment: Assessment and Control, November 13 - 16, 1995, Dearborn, MI, pp 396 - 401

Amy B. Dindal, C.Y. Ma, Roger A. Jenkins, Cecil E. Higgins, J. Todd Skeen, and Charles K. Bayne, "Application of Multisorbent Traps to Characterization and Quantification of Workplace Exposure Source Terms," Proceedings of the 1995 EPA/AWMA Conference on the Measurement of Toxic and Related Air Pollutants, Raleigh, NC, May 16 - 18, 1995, pp. 391 - 396

R. A. Jenkins, C. W. Nestor, C. V. Thompson, T. M. Gayle, C. Y. Ma, B. A. Tomkins, and R. L. Moody, "Characterization of Rocket Propellant Combustion Products: Chemical Characterization and Computer Modeling of the Exhaust Products from Four Propellant Formulations," Final Report ORNL/TM-11759, April 1992.

Roger A. Jenkins, Jack H. Moneyhun, Tom M. Gayle, James D. Lore, Robert H. Ross (1988) Problem Definition Study On Techniques And Methodologies For Evaluating The Chemical And Toxicological Properties Of Combustion Products Of Gun Systems: Facility Criteria for the Chemical and Toxicological Characterization of Gun Exhaust, FINAL REPORT ORNL 6334 Available through the National Technical Information service, Springfield, VA

R. A. Jenkins, W. H. Griest, J. H. Moneyhun, B. A. Tomkins, R. H. Ilgner, C. E. Higgins, and T. M. Gayle, "Sampling and Chemical Characterization of Workplace Atmospheres Contaminated with Airborne Diesel Exhaust," Proceedings of the 1988 EPA/APCA Symposium on Measurement of Toxic and Related Air Pollutants, May 2-4, 1988, Quality-Mission Valley, Raleigh, NC. pp. 119-130

J. H. Moneyhun, T. M. Gayle, and R. A. Jenkins, "A Laboratory Scale Liquid/Solid Smoke Generator to Simulate the XM55 Field System," Proceedings of the 12th Annual Smoke/Obscurants Symposium, April 19-21, 1988, John Hopkins University, Laurel, MD.

R. A. Jenkins, R. W. Holmberg, J. S. Wike, J. H. Moneyhun, and R. S. Brazell, "Chemical and Physical Characterization of Diesel Fuel Smoke," ORNL/TM-9196, June 1984, 69 pp.

R. A. Jenkins, D. L. Manning, M. P. Maskarinec, J. H. Moneyhun, W. Dalbey, and S. Lock, "Diesel Fuel Smoke Particulate Dosimetry in Sprague-Dawley Rats," ORNL/TM-9195, June 1984, 49 pp.

R. A. Jenkins, T. M. Gayle, J. S. Wike, and D. L. Manning, "The Sampling and Chemical Characterization of Concentrated Smokes," in Toxic Materials in the Atmosphere, ASTM STP 786, American Society for Testing and Materials, 1982, p. 153.


Development of Analytical Methods for Trace Environmental Contamination

Bruce A. Tomkins and Ralph H. Ilgner, "Determination of Atrazine and Four Organophosphorous Pesticides in Ground Water Using Solid Phase Microextraction (SPME) Followed by Gas Chromatography with Selected-Ion Monitoring", Journal of Chromatography A, 972, 183-194 (2002).

Bruce A. Tomkins and Angela R. Barnard, "Determination of Organochlorine Pesticides in Ground Water Using Solid-Phase Microextraction (SPME) Followed by Dual-Column Gas Chromatography with Electron Capture Detection", Journal of Chromatography A, 964, 21-33 (2002).

Bruce A. Tomkins and Gary A. Sega, "Determination of Thiodiglycol in Groundwater Using Solid Phase Extraction Followed by Gas Chromatography with Mass Spectrometric Detection in the Selected Ion Mode", in Proceedings of the 2001 Scientific Conference on Chemical & Biological Defense Research, 6-8 March 2001, Hunt Valley, MD, available on CD ROM.

B. A. Tomkins and Gary A. Sega, "Determination of Thiodiglycol in Groundwater Using Solid Phase Extraction Followed by Gas Chromatography with Mass Spectrometric Detection in the Selected Ion Mode," Journal of Chromatography A, 911, 85-96 (2001).

B. A. Tomkins, G. A. Sega, and C-h. Ho, "The Determination of Lewisite Oxide in Soil Using Solid Phase Microextraction: An Example of a New 'Green' Analytical Procedure", Proceedings of the American Society for Quality Energy and Environmental Division 2000 Energy and Environmental Conference, August 27-30, 2000, Tucson OMNI Hotel, Tucson, AZ, pp. 128-149. Available on CD-ROM.

B. A. Tomkins, "Explosives Analysis in the Environment", a chapter in Robert A. Meyers, ed., Encyclopedia of Analytical Chemistry, Chichester, John Wiley & Sons, Ltd., 2000, pp. 2402-2441.

B. A. Tomkins, Gary A. Sega, and C-h. Ho, "Determination of Lewisite Oxide in Soil Using Solid Phase Microextraction Followed by Gas Chromatography With Flame Photometric or Mass Spectrometric Detection" Journal of Chromatography A, 909, 13-28 (2001).

B. A. Tomkins , G. A. Sega , and S. J. Macnaughton, "The Quantitation of Sulfur Mustard By-Products, Sulfur- Containing Herbicides, and Organophosphonates in Soil and Concrete", Analytical Letters, 31(9), 1603-6122 (1998).

G. A. Sega, W. H. Griest, B. A. Tomkins, and C. K. Bayne, "The Hydrolysis of Di-isopropyl Methylphosphonate in Groundwater", Journal of Environmental Science and Health, Part A (Environmental Science and Engineering & Toxic and Hazardous Substance Control), A33(2), 213-236 (1998).

B. A. Tomkins, G. A. Sega, and S. J. MacNaughton, The Quantitation of Sulfur Mustard By-products and Two Sulfur-containing Herbicides in Soil and Concrete, Proceedings of the 1997 U. S. Army Edgewood Research, Develoment and Engineering Center, Scientific Conference on Chemical and Biological Defense Research, Edgewood Area Conference Center, Aberdeen Proving Ground, MD, November 18-21, 1997.

G. A. Sega, B. A. Tomkins, W. H. Griest, and C. K. Bayne, The Hydrolysis of Di-isopropyl Methylphosphonate in Groundwater, Proceedings of the 1997 U. S. Army Edgewood Research, Develoment and Engineering Center, Scientific Conference on Chemical and Biological Defense Research, Edgewood Area Conference Center, Aberdeen Proving Ground, MD, November 18-21, 1997.

G. A. Sega, B. A. Tomkins, and W. H. Griest, Analysis of Methyl Phosphonic Acid, Ethyl Methyl Phosphonic Acid and Isopropyl Methyl Phosphonic Acid at Low Microgram per Liter Levels in Groundwater, Journal of Chromatography A, 790, 143-152 (1997).

B. A. Tomkins, W. H. Griest, and D. R. Hearle, "Determination of Small Dialkyl Organophosphonates at Microgram/L Concentrations in Contaminated Groundwaters Using Multiple Extraction Membrane Disks", Analytical Letters, 30(9), 1697-1717 (1997).

B. A. Tomkins, W. H. Griest, and C. E. Higgins, "Determination of N-Nitrosodimethylamine at Part-Per-Trillion Levels in Drinking Waters and Contaminated Groundwaters", Proceedings of the 18th Annual EPA Conference on Analysis of Pollutants in the Environment, Marriott Waterside Hotel, Norfolk, VA, May 3-4, 1995. U. S. Environmental Protection Agency, Office Water, document no. EPA-821-H-96-001, received May 12, 1997. Slide presentation pp. 203-209. Text given on accompanying floppy disk, document no. EPA-821-H-96-009, pp. 253-269.

B. A. Tomkins, W. H. Griest, G. Connolly, and H. C. Hayes, "Determinations of N-nitroso-dimethylamine (NDMA) at Part-per-Trillion (ng/L) Concentrations in Contaminated Groundwaters and Drinking Waters Featuring Carbon-based Membrane Extraction Disks", Proceedings of the Twelfth Annual Waste Testing and Quality Assurance Symposium, July 23-23, 1996, Washington Hilton & Towers, Washington, D.C., pp. 423-431.

B. A. Tomkins and W. H. Griest, "Determinations of N-Nitrosodimethylamine (NDMA) at Part-Per-Trillion (ng/L) Concentrations in Contaminated Groundwaters and Drinking Waters Featuring Carbon-Based Membrane Extraction Disks", Analytical Chemistry, 68 (15), 2533-2540 (1996).

B. A. Tomkins, W. H. Griest, and C. E. Higgins, "Determination of N-Nitrosodimethylamine (NDMA) at Part-Per-Billion (ng/L) Levels in Drinking Waters and Contaminated Groundwaters", Analytical Chemistry, 67(23), 4387-4395 (1995).

B. A. Tomkins, "Screening Procedure for Sodium Fluoroacetate (Compound 1080) at Sub-Microgram/Gram Concentrations in Soils", Analytical Letters, 27(14), 2703-2718 (1994).

B. A. Tomkins, R. Merriweather, R. A. Jenkins, and Charles K. Bayne, "Determination of Eight Organochlorine Pesticides at Low ng/L Concentrations in Groundwater Using Filter Disk Extraction and Gas Chromatography", Journal of AOAC International, 75(6), 1091-1099 (1992).

W. H. Griest, R. S. Ramsey, C-h. Ho, and W. M. Caldwell, "Supercritical Fluid Extraction and Organic Solvent Extraction of Chemical Warfare Agent Simulants from Soil," Proceedings of the U. S. Army Chemical Conference on Chemical Defense Research, ERDEC-SP-002, June, 1993, pp. 257-263.

W. H. Griest, R. S. Ramsey, C-h. Ho, and W. M. Caldwell, "Supercritical Fluid Extraction of Chemical Warfare Agent Simulants from Soil," J. of Chromatography, 600, 273-277 (1992).

Oral Presentations:

Bruce A. Tomkins, Gary A. Sega, and Angela R. Barnard, "Solid-Phase Microextraction: An Application of 'Green' Analytical Chemistry to the Clean-up of the U. S. Army Rocky Mountain Arsenal", an invited seminar presented to the Department of Chemistry, School of Chemical Sciences, University of Illinois at Urbana-Champaign, Urbana, IL, April 2, 2002.

Bruce A. Tomkins and Gary A. Sega, "Determination of Thiodiglycol in Groundwater Using Solid Phase Extraction Followed by Gas Chromatography with Mass Spectrometric Detection in the Selected Ion Mode", presented to the 2001 Scientific Conference on Chemical & Biological Defense Research, 6-8 March 2001, Hunt Valley, MD.

B. A. Tomkins, Gary A. Sega, and C-h. Ho, "The Determination of Lewisite Oxide in Soil Using Solid Phase Microextraction: An Example of a New "Green" Analytical Procedure", presented to American Society for Quality Energy & Environmental Division 2000 Energy and Environmental Conference, Tucson OMNI Hotel, Tucson, AZ, August 27-30, 2000. INVITED PRESENTATION.

B. A. Tomkins, Gary A. Sega, and C-h. Ho, "Determination of Lewisite Oxide in Soil Using Solid Phase Microextraction Followed by Gas Chromatography With Flame Photometric or Mass Spectrometric Detection", presented to ExTech® 2000, May 1-3, 2000, University of Waterloo, Ontario, Canada.

B. A. Tomkins, G. A. Sega, S. J. Macnaughton, "The Quantitation of Sulfur Mustard By-products and Two Sulfur-containing Herbicides in Soil and Concrete", presented to the 1997 Scientific Conference on Chemical and Biological Defense Research, Aberdeen Proving Ground, MD, November 18-21, 1997.

G. A. Sega, B. A. Tomkins, W. H. Griest, and C. K. Bayne, "The Hydrolysis of Di-isopropyl Methylphosphonate in Groundwater", presented to the 1997 Scientific Conference on Chemical and Biological Defense Research, Aberdeen Proving Ground, MD, November 18-21, 1997

B. A. Tomkins, W. H. Griest, G. Connolly and H. C. Hayes, "Determinations of N-Nitrosodimethylamine (NDMA) at Part-Per-Trillion (ng/L) Concentrations in Contaminated Groundwaters and Drinking Waters Featuring Carbon-Based Membrane Extraction Disks", presented to the 12th Annual Waste Testing & Quality Assurance Symposium, July 23-26, 1996, at the Washington Hilton & Towers in Washington, D. C.

B. A. Tomkins, W. H. Griest, and C. E. Higgins, "Determination of N-Nitrosodimethylamine (NDMA) at Part-Per-Trillion (ng/L) Levels in Drinking Waters and Contaminated Groundwaters", presented to the 18th Annual Conference on the Analysis of Pollutants in the Environment, Norfolk Waterside Marriott, Norfolk, VA, May 3-4, 1995.

B. A. Tomkins, "The Challenge of Quantitating Ultratrace Concentrations of Water-Miscible Polar Neutrals in Groundwaters", presented to the 35th ORNL-DOE Conference on Analytical Chemistry in Energy Technology, Park Vista Hotel, Gatlinburg, TN, October 11-13, 1994. Solicited paper. CONF-9410147.

B. A. Tomkins, R. A. Jenkins, R. Merriweather, and C. E. Higgins, "Solid Sorbent Technology for the Determination of Organic Pollutants in Soil, Air, and Water", poster presented to the Analytical Chemistry Division Information Meeting, March 18, 1992, Garden Plaza Hotel, Oak Ridge, TN.

B. A. Tomkins, R. Merriweather, and R. A. Jenkins, "Analysis of Eight Organochlorine Pesticides at Low Part-per-Trillion Concentrations in Groundwater", poster presented to the 105th AOAC Annual International Meeting and Exposition, The Pointe on South Mountain, Phoenix, AZ, August 12-15, 1991; presentation no. 318.

C. -h. Ho, W. H. Griest, R. S. Ramsey, and W. M. Caldwell, "Supercritical Fluid and Microsolvent Extraction of Chemical Warfare Agent Simulants from Soil," Scientific Conference on Chemical Defense Research, U. S. Army Chemical Research, Development and Engineering Center, Aberdeen Proving Ground, MD, November 19-22, 1991.


Energy Efficient Process and Materials Chemistry


Environmental Tobacco Smoke Characterization and Exposure

Roger A. Jenkins, Michael P. Maskarinec, Richard W. Counts, John E. Caton, Bruce A. Tomkins, and Ralph H. Ilgner (2001) "Environmental Tobacco Smoke (ETS) in an Unrestricted Smoking Workplace: Area and Personal Exposure Monitoring" Journal of Exposure Analysis and Environmental Epidemiology, 11: 369 - 380

Sung-Ok Baek and Roger A Jenkins (2001) "Performance Evaluation of Simultaneous Monitoring of Personal Exposure to Environmental Tobacco Smoke and Volatile Organic Compounds" Indoor and Built Environment, 10: 200 - 208

Roger A. Jenkins, Derrick Finn, Bruce A. Tomkins, and Michael P. Maskarinec, (2001) "Environmental Tobacco Smoke in the Non-Smoking Section of a Restaurant: A Case Study" Regulatory Toxicology and Pharmacology, 34: 213 - 220

Roger A. Jenkins "Commentary: Don't Hold Your Breath" Preventive Medicine, 31: 629 - 630, 2000

Roger A. Jenkins, M. P. Maskarinec, John E. Caton, Richard W. Counts and Bruce A. Tomkins, R. H. Ilgner, (2000) "Personal Exposure to Environmental Tobacco Smoke in a Demographically Representative Subject Population" presented at the International Society of Exposure Analysis Conference, Monterey, CA October 24 ? 27, 2000

Gevecker Graves, C.,Ginevan, M. E., Jenkins, R. A., Tardiff, R. G.. (2000). "Doses and lung burdens of environmental tobacco smoke constituents in nonsmoking workplaces." J Expo Anal Environ Epidemiol 10(4): 365?77.

Jenkins, R.A., Guerin, M.R., and Tomkins, B.A., The Chemistry of Environmental Tobacco Smoke: Composition and Measurement, Second Edition, Lewis Publishers, Boca Raton, FL, 467 pp, 2000

Maskarinec, M.P., Jenkins, R.A., Counts, R.W., and Dindal, A.B., "Determination of Exposure to Environmental Tobacco Smoke in Restaurant and Tavern Workers in One US City" Journal of Exposure Analysis and Environmental Epidemiology,10, 36 - 49, 2000

Ogden, M.W. and Jenkins, R.A., "Nicotine in Environmental Tobacco Smoke" in Analytical Determination of Nicotine and Related Compounds and their Metabolites, John W. Gorrod and Peyton Jacob III, editors, Elsevier Amsterdam, 1999

Jenkins, RA and Counts R.W., "Occupational Exposure to Environmental Tobacco Smoke: Results of Two Personal Exposure Studies" Environmental Health Perspectives 107 Suppl 2 341 - 348, 1999

Jenkins, R.A and Counts, R.W.,"Personal Exposure to Environmental Tobacco Smoke: Salivary Cotinine, Airborne Nicotine, and Non?smoker Misclassification", Journal of Exposure Analysis and Environmental Epidemiology, 9, 352 - 363, 1999

LaKind JS, Jenkins RA, Naiman DQ, Ginevan ME, Graves CG, Tardiff RG. "Use of Environmental Tobacco Smoke (ETS) Constituents as Markers for Exposure." Risk Analysis: An International Journal, 19 (3) 359 - 373,1999

LaKind JS, Graves CG, Ginevan ME, Jenkins RA, Naiman DQ, and Tardiff RG "Exposure to Environmental Tobacco Smoke in the Workplace and the Impact of Away?from?work Exposure" Risk Analysis: An International Journal, 19 (3) 349 - 358, 1999

LaKind JS, Ginevan ME, Naiman DQ, James AC, Jenkins RA, Dourson ML, Felter SP, Graves CG, and Tardiff RG "Distribution of Exposure Concentrations and Doses for Constituents of Environmental Tobacco Smoke" Risk Analysis: An International Journal 19 (3), 375 - 390, 1999

Roger A. Jenkins, Andi Palausky, Richard W. Counts, Charles K. Bayne,Amy B. Dindal, and Michael R. Guerin, "Exposure to Environmental Tobacco Smoke in Sixteen Cities in the United States As Determined by Personal Breathing Zone Air Sampling," Journal of Exposure Analysis and Environmental Epidemiology, 6,(4) 473 - 502, 1996

Roger A. Jenkins, "Methodological Considerations for the Study of Human Exposure to Environmental Tobacco Smoke," Tumor (Shanghai), 16, 480 - 486, 1996

Roger A. Jenkins, Andi Palausky, Richard W. Counts, Michael R. Guerin, Amy. B. Dindal, and Charles K. Bayne, "Determination of personal exposure to environmental tobacco smoke in the United States," Lung Cancer, 14 Suppl. 1, S195 - S213, 1996

Stephen V. Teague, Kent E. Pinkerton, Michael Goldsmith, Assefa Gebremichael, Sharon Chang, Roger A. Jenkins, and Jack H. Moneyhun, "Sidestream Cigarette Smoke Generation and Exposure System for Environmental Tobacco Smoke Studies," Inhalation Toxicology, 6, 79 - 93, 1994

R. S. Ramsey, J. H. Moneyhun, and R. A. Jenkins, "Generation , sampling, and chromatographic analysis of particulate matter in dilute sidestream tobacco smoke," Analytica Chimica Acta, 236, 213 - 220, 1990

C. V. Thompson, R. A. Jenkins, and C. E. Higgins, "A Thermal Desorption Method for the Determination of Nicotine in Indoor Environments," Environmental Science & Technology, 23, pp. 429-435, April 1989

M. R. Guerin, C. E. Higgins and R. A. Jenkins, "Measuring Environmental Emissions from Tobacco Combustion: Sidestream Cigarette Smoke Literature Review," Atmospheric Environment, Vol. 21, No. 2, pp. 291-297, 1987.

Cecil E. Higgins, Roger A. Jenkins, and Michael R. Guerin, "Organic Vapor Phase Composition of Sidestream and Environmental Tobacco Smoke from Cigarettes," Proceedings of the 1987 EPA/APCA Symposium on Measurement of Toxic and Related Air Pollutants, pp. 140-145, 1987

T. L. Guidotti, S. Binder, J. W. Stratton, F. G. Schecter, and R. A. Jenkins, "Clove Cigarettes: Development of the Fad and Evidence for Health Effects," Current Topics in Pulmonary Pharmacology and Toxicology, Mannfred A. Hollinger, ed., Vol. 2, pp. 1-23 (1987).

B. A. Tomkins, R. A. Jenkins, W. H. Griest, R. R. Reagan, and S. K. Holladay, "Liquid Chromatographic Determination of Benzo(a)pyrene in the Total Particulate Matter of Cigarette Smoke," J. Assoc. Off. Anal. Chem. 68, 935 (1985).

R. A. Jenkins, "Occurrence of Selected Metals in Cigarette Tobaccos and Smoke," Environmental Carcinogens - Selected Methods of Analysis - Volume 8 - Some Metals, International Agency for Research on Cancer, Lyon, France, IARC Scientific Publications No. 71, 1986, pp. 129-138.

J. Nolan, R. A. Jenkins, K. Kurihara, and R. C. Schultz, "The Acute Effects of Cigarette Smoke Exposure on Experimental Skin Flaps," Plastic and Reconstructive Surgery, 75, 544 (1985).

B. A. Tomkins, R. A. Jenkins, W. H. Griest, R. R. Reagan, and S. K. Holladay, "Liquid Chromatographic Determination of Phenol and Cresols in Total Particulate Matter of Cigarette Smoke," J. Assoc. Off. Anal. Chem., 67(5), 919 (1984).

R.S. Brazell, A.C. Stiff, G.M. Henderson, R.A. Jenkins, P.L. Romig, and O. Auerbach, "Plasma Nicotine and Cotinine in Tobacco Smoke Exposed Beagle Dogs," Toxicology and Applied Pharmacology, 73, 152 - 158 (1984)

R. A. Jenkins and M. R. Guerin, "Analytical Chemical Methods for the Detection of Environmental Tobacco Smoke Constituents," Eur. J. of Res. Dis., Supplementum No. 133, Vol. 65, 33 (1984).

R. A. Jenkins and T. M. Gayle, "An Instrumental Cigarette Smoke Monitor Designed for the Direct Measurement of Smoke Particulate Matter Generated in Human Smoking Studies," Behavior Res. Methods. Instrum. and Computers, 16(3), 263 (1984).

R. S. Brazell, C. K. Bayne, and R. A. Jenkins, "Profile Analysis of Organic Volatiles in Urine of Tobacco Smoke-Exposed Beagles," Anal. Chim. Acta, 139, 247 (1982).

R. A. Jenkins and B. E. Gill, "Determination of Oxides of Nitrogen (NOx) in Cigarette Smoke by Chemiluminescent Analysis," Anal. Chem., 52(6), 925 (1980).


Characterization of Explosives and Associated Residues in Environmental and Forensic Media

M.E. Sigman and R. H. Ilgner "Operational Guideline: Tenax TA® Collection and In-Injection Port Thermal Desorption Analysis of Trace Levels of Organic Explosive Vapors" ORNL/TM-2001/162   Available through the National Technical Information Service.

Michael E. Sigman, Cheng-Yu Ma, and Ralph H. Ilgner, "Performance Evaluation of an In-Injection Port Thermal Desorption/Gas Chromatographic/Negative Ion Chemical Ionization Mass Spectrometric Method for Trace Explosive Vapor Analysis," Anal. Chem., 73 (4), 792 -798, 2001

Michael E. Sigman and Cheng-Yu Ma, "Detection Limits for GC/MS Analytis of Organic Explosives J. Forensic Sci; 46: 6-11, 2001


Field Analytical Development Application and Performance Verification

Amy Dindal, Roger Jenkins, Chuck Bayne, Wayne Einfeld, Karen Riggs, and Eric Koglin, "Performance Verification of Field Analytical Technologies That Can Assist in Site Characterization and Monitoring Activities," presented at ER TEC 2001, Atlanta, GA, July 18, 2001.

Roger A. Jenkins and Joe Rossabi, "True Grit ? True Costs, True Needs and Other Realities of Long-Term Monitoring," Presented at the Long Term Monitoring Sensors/Analytical Methods Workshop, Orlando, FL, June 13 - 15, 2001 Invited

Dindal, A., C. Bayne, R. Jenkins, and E. Koglin, "Environmental Technology Verification Report, PCB Detection Technology, Hybrizyme DELFIA PCB Assay," EPA Report EPA/600/R?01/052, August 2001.

Dindal, A., C. Bayne, R. Jenkins, and E. Koglin, "Environmental Technology Verification Report, PCB Detection Technology, Dexsil Corporation L2000DX Analyzer," EPA Report EPA/600/R?01/049, August 2001.

Charles K. Bayne, Amy B. Dindal, Roger A. Jenkins, Deana Crumbling, and Eric N. Koglin, (2001) "Meeting Data Quality Objectives with Interval Information", Environmental Science & Technology, 35 (16): 3350?3355

Roger Jenkins, Amy Dindal, Wayne Einfeld, Charles Bayne, Deana Crumbling, and Eric Koglin, "Performance Verification of Field Analytical Technologies that Can Assist in Site Characterization and Monitoring Activities," Presented at the Green Brownfields Conference, Salt Lake City, March 19 - 23, 2000

Amy B. Dindal Charles K. Bayne, Roger A. Jenkins, Eric N. Koglin "Environmental Technology Verification Report Explosives Detection Technology Research International, Inc. FAST 2000 EPA/600/R?00/045 March 2000

Amy B. Dindal Charles K. Bayne, Roger A. Jenkins, Eric N. Koglin "Environmental Technology Verification Report Explosives Detection Technology Barringer Instruments IONSCAN EPA/600/R?00/046 March 2000

Sullivan, T., A. Armstrong, A. Dindal, C. Bayne, R. Jenkins, J. Osleeb, and E. Koglin, "Environmental Technology Verification Report, Environmental Software - SitePro Version 3.0," EPA Report EPA/600/R?99/093, October 1999.

Sullivan, T., A. Armstrong, A. Dindal, C. Bayne, R. Jenkins, J. Osleeb, and E. Koglin, "Environmental Technology Verification Report, Environmental Systems Research Institute - ArcView GIS Version 3.1," EPA Report EPA/600/R?99/094, October 1999.

Sullivan, T., A. Armstrong, A. Dindal, C. Bayne, R. Jenkins, J. Osleeb, and E. Koglin, "Environmental Technology Verification Report, University of Tennessee Research Corporation - Spatial Analysis and Decision Assistance (SADA)" EPA Report EPA/600/R?00/036, February 2000.

Dindal, A., C. Bayne, R. Jenkins, and E. Koglin, "Environmental Technology Verification Report, EnviroLogix - PCB In?Soil Tube Assay," EPA Report EPA/600/R?98/1173, December 1998.

Dindal, A., C. Bayne, R. Jenkins, and E. Koglin, "Environmental Technology Verification Report, Electronic Sensor Technology - Model 4100 Vapor Detector," EPA Report EPA/600/R?98/114, August 1998.

Larry C. Waters, Andi Palausky, Richard W. Counts, and Roger A. Jenkins, "Experimental Evaluation of Two Field Test Kits for the Detection of PAHs by Immunoassay," Field Analytical Chemistry and Technology, 1(4) 227 - 238, 1997

Larry C. Waters, M.A. Palausky, Richard W. Counts, and Roger A. Jenkins, "Performance of Commercially Available Immunoassay-Based Field Test Kits for Petroleum Fuel Hydrocarbons in Soil, Field Analytical Chemistry and Technology, 1(3) 135 - 144, 1997

Larry C. Waters, Richard W. Counts, Rob R. Smith, and Roger A. Jenkins, "Studies on the Applications of an Immunoassay for Mercury," in Immunochemical Technology for Environmental Applicaitons, ACS Symposium Series 657, 280 - 289, 1997

Olivia R. West, Robert L. Siegrist, Toby J. Mitchell, and Roger A. Jenkins, "Measurement Error and Spatial Variability Effects on Characterization of Volatile Organics in the Subsurface," Environmental Science and Technology, 29, 647 - 656, 1995

Roger A. Jenkins, Cecil E. Higgins, Tom M. Gayle, G. Wilbur Allin, and Rob R. Smith, "Field Experiences with a Multisorbent Arrayed Sampler for In-situ Collection of Vadose Zone Volatile Organic Compounds," Proceedings of the 1995 EPA/AWMA International Symposium on Methods for the Screening of Hazardous Wastes and Toxic Chemicals, Las Vegas, February, 1995, pp 1018 - 1024

Mary A. Palausky, Larry C. Waters, Richard W. Counts, and Roger A. Jenkins, "Adapting the Bruel & Kjaer Multi-gas Monitor Type 1302 to Measure Selected Volatile Organic Chemicals (VOCs) in Soil," Presented at the International Symposium for Field Screening Methods for Hazardous Wastes and Toxic Chemicals, Las Vegas, NV, February, 1995

Charles K. Bayne, Denise D. Schmoyer, and Roger A. Jenkins, "Practical Reporting Times for Environmental Samples," Environmental Science & Technology, 28, 1430 - 1436, 1994

M. P. Maskarinec, L. H. Johnson, S. K. Holladay, R. L. Moody, C. K. Bayne,and R. A. Jenkins, "Stability of Volatile Organic Compounds in Environmental Water Samples During Transport and Storage," Environmental Science & Technology, 24, 1665 - 1670, 1990

R. A. Jenkins, F. F. Dyer, R. L. Moody, C. K. Bayne, and C. V. Thompson, "Experimental Evaluation of Selected Field Portable Instrumentation for the Quantitative Determination of Contaminant Levels in Soil and Water at Rocky Mountain Arsenal - FINAL REPORT," ORNL/TM-11385, October 1989


More information to come!

Applied Technology Group

Provided by Oak Ridge National Laboratory's Chemical Sciences Division
Rev:   June 26, 2003